3大葱籽黑色素提取工艺研究.pdfVIP

, Journ l ofAnhuiAgr.i Sci. 2010, 38( 13) : 7162- 7164 王强 卢瑶 鲁京兰, 崔成都, 南昌熙 (, 133400) [目的]研究大葱籽黑色素提取工艺, 为其药学研究和开发利 提供理论依据[方法] 以大葱籽为原料, 从中提取黑色素, 并进 行纯化, 研究提取条件, 确定最佳工艺[结果] 大葱籽黑色素的最佳提取工艺条件为: 盐酸浓度 11mol/L,料液比为 140, 水解温度为55 , 水解时间 3 h[结论]盐酸浓度是影响大葱籽黑色素提取率的最主要因素, 其次是水解时间温度和料液比 大葱籽; 黑色素; 提取工艺 S633. 1 A 0517- 6611( 2010) 13- 07162- 03 Ex traction P rocess ofM elanin from Ch inese On ion Seeds LU J inglan et al ( Agricultur lCollege ofY nb i n U niversity, Longjng, Jilin 133400) A bstract [ Objective] To study the extr ction process of onion seed mel nin, nd prov ide theoretic l b sis for Chinese onion ph rm ceuti c l rese rch nd utiliz tion. [M ethod] Onion seeds were used s test m teri ls. The ex tr ction nd pur ific tion ofm el nin were perform ed, nd the optmi um conditions were determ ined. [ Result] The optmi um ex tr ction conditions of Onion seedsm el nin were s follows: the con centr tion of hydrochlor ic cid w s 11mol/L, solidliquid r tiow s 140, the hydrolysis temper turew s 55 , nd the hydrolysis tmi ew s 3 h. [ Conclusion] Thehydroch loric cid concentr tion is them ost mi port nt f ctor ffectingm el nin extr ction of on ion seeds, follow ed by the hydrolysis tmi e, temper ture nd solidliquid r tio. K ey w ords Onion seeds; M el nin; Extr ction process (M el nin) TDL5000B(); [ 1] , , FA /JA (); PHS3C , pH(); , 2 (); 756MC ; ; (); ( [2] , ) , 1 3 , 1. 000 0 g, 150 ml, 75 ml 6mol/L HCl [ 3] , , 75 5 h; , , , : , 70 g/L N OH 400m l, [ 4] , 12 h, 6mol/LHC l pH 1,