伏格列波糖溶出度 JP.pdfVIP

Supplement I, JP XVI Official Monographs Assay Weigh accurately the mass of not less than 20 Val- sartan Tablets, and powder. Weigh accurately a portion of Vasopressin Injection the powder, equivalent to about 50 mg of valsartan (C H N O ), add 60 mL of the mobile phase, shake thor- バソプレシン注射液 24 29 5 3 oughly, add the mobile phase to make exactly 100 mL, and centrifuge. Pipet 5 mL of the supernatant liquid, add exactly Change the Assay (ii) as follows: 3 mL of the internal standard solution, add the mobile phase Assay to make 50 mL, and use this solution as the sample solution. (ii) Standard stock solution: Dissolve 2000 Units of Separately, weigh accurately about 50 mg of Valsartan RS Vasopressin RS, according to the labeled Units, in exactly (separately, determine the water 2.48 and the residual sol- 100 mL of diluted acetic acid (100) (1 in 400). Pipet 1 mL of vent in the same manner as Valsartan), and dissolve in the this solution, and add diluted acetic acid (100) (1 in 400) to mobile phase to make exactly 100 mL. Pipet 5 mL of this so- make exactly 10 mL. lution, add exactly 3 mL of the internal standard solution, add the mobile phase to make 50 mL, and use this solution as the standard solution. Perform the test with 10 mL each of Voglibose Tablets the sample