_竹林胺_中有效成分的一阶导数光谱法测定.pdf

Journal of Zhengzhou University Medical Sciences) Jan. 2004 Vol . 39 No. 1 # 121 # ! 1) ∀ 2) 3) 曹书霞 戴晓弘 韩华云 1) 4 50052 2) 450001 3) 4 50052 ∀ , 35 , , , : 关键词 ; ; ; 中图分类号 R917 摘要 : ! : , 267 nm270 nm , - ! : ! 99. 34% , , , Determination of phenoxybenzamine hydrochloriod in Zhulinan! tablets by the first derivative ultraviolet spectrophotometry 1 ) 2 ) 3 ) CA O Shuxia , DAI X iaohong , HAN H uayun 1) Dep artment of Chemistry , Zheng hou University , Zheng hou 450052 2 ) Henan Joyline Joysun Pharma ceutical Stock Co . Ltd, Zheng hou 450001 3 ) Dep artment of Chemistry , Zheng hou Universty , Zheng hou 450052 Key words f irst derivative ultraviolet spectrophotometry ; zhulinan ; phenoxybenzamine hydrochloriod ; analysis Abstract Aim: To develop a method for determining the content of phenoxybenzamine hydrochloriod in zhulinan! tablets. Methods: The first derivative ultraviolet spectrophotometry w as used for determination. The w avelength of the pair of determinated w aves w as 267 nm and 270 nm. The content of phenoxybenzamine hydrochloriod in zhulinan! tablets w as determined by peak- valley method . Result s and Conclusions: The method is rapid and simple. The recovery of phenoxybenzamine hydrochloriod in zhulinan! tablets is 99. 34% . The accuracy and precision meet the requirements of the pharmaceutical preparations analysis . ! - , , , , Phenoxybenzamine Hydrochloride) , ! [ 1] 1 , , 1. 1 HP 8453 , ) ; : ! ; ! : patitis B virus DNA in serum and liver from patients w ith chronic ral hepatitis despite active