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氮化钽薄膜的制备与结构研究.pdf
/ 19989
*
Research on Synthesis of Taltanlum Nitride Film and Its Structure
()
Leng YongxiangHuang NanYang Ping
( ept of Materials Engineering Southwest Jiaotong University. , )
[ ] , TEM XR
: ; ( 16nm ) ; , ,
, , ,
2
4000kg/ mm ,
[ Abstract] T he taltanlum nitride film has been deposited by the reactive magnetron sput-
tering. T he microstructure of the film were characterize by XR and T EM techniques.T he re-
sults revealed that the multiphase was coexistent in the film and the grain size of the film was
small ( about 16nm) . In addition, the preferred orientation was observed, and it changed and de-
2
veloped along the direction where the interplanar spacing was more broad when increasing N par-
tial pressure. Synthesized under specific conditions the hardness of the taltanlum nitride film
4000 / 2 . .
reached kg mm or above The cause of high hardness of the film was discussed The cause
2
of the preferred orientation changed when increasing N partial pressure was also discussed.
Keywords taltanlum nitride film hardness microstructure
1 , 60mm; 710- 3
Pa; , 200
, TaN T a N
2 1
,
[ 1, 2] 1 -
, Ta N
2 T able 1M anufacturing process of the T a-N film
[ 3] 4100kgf/ mm ,
, Pa , Pa , W
, ,
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