紫外分光光度法测定水质总氮的影响因素分析.docVIP

紫外分光光度法测定水质总氮的影响因素分析 张正美 （南京市江宁区环境监测站） 摘要：通过实验数据比对，对实验用水、消解温度与时间、冷却时间等影响总氮测定的因素进行分析。实验结果表明,新鲜一次蒸馏水和新鲜去离子水可代替重蒸馏无氨水；在消解温度122℃，消解时间50min，冷却时间2~3h的条件下，测量结果最佳。 关键词：碱性过硫酸钾氧化；总氮；紫外分光光度法；影响因素 Analysis of the influence factors of the determination of total nitrogen in water and waste water by using UV spectrophotometry Abstract: In this paper, some factors that had great impact on the accuracy and precision of the determination of total nitrogen in water and waste water by using the alkaline potassium persiflage digestion – UV spectrophotometric method (GB11894-1989). These factors included the exper