广西山银花的质量的分析.pdfVIP

8 2．2．3检测波长的选择………………………………·…1 1 2．2．4流速的选择．．……………………_………一·…2 1 2．2．5色谱条件的确定·······························一·······2 2．3 药材供试品的制备……………………………···…22 2 2．3．1提取溶剂的考察··················…···············-···2 3 2．3．2提取方法的考察······································．·2 4 2．3．3供试品的制备…………………一……………·…2 4 2．4参照物的选择···········································2 2．5方法验证·····························一-···一··········25 5 2．5．1稳定性试验…………………一……………···…2 6 2．5．2精密度试验…………………………………·。…2 7 2．5．3重复性试验…………………………………··…2 9 2．6广西红腺忍冬HPLC指纹图谱…···……·······…··一．．··2 9 2．6．1红腺忍冬样品HPLC指纹图谱……一……………···…2 5 2．6．2红腺忍冬标准指纹图谱…………………………·…3 2．6．3相似度计算·……………………一…………··…35 3广西不同产地、不同加工方法红腺忍冬中绿原酸的含量测 定·························································37 7 3．1仪器、材料与试剂………一…………．…………·…3 7 3．1．1仪器·················“············一·················3 7 3．I．2材料与试剂··……······…········…················3