《Selective removal of heavy metal ions from aqueous solutions with surface functionalized silica nanoparticles by different functional groups.》.pdf
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《Selective removal of heavy metal ions from aqueous solutions with surface functionalized silica nanoparticles by different functional groups.》.pdf
J.Cent.SouthUniv.(2014)21:3575—3579 垒Springer
D0I:10.1007/sl1771—014.2338.0
Selectiveremovalofheavymetalionsfrom aqueoussolutionswith
surfacefunctionalizedsilicananoparticlesbydi rentfunctionalgroups
KONGXiang—feng(孔祥峰),一,YANGBin(杨斌) ,XIONGHeng(~恒) ,ZHOUYang(周阳)一,
XUESheng.guo(~ N),xuBao.qiaIlg(徐宝强)一,WANGShi.xing(王世兴)
1.NationalEngineeringLaboratoryforVacuumMetallurgy(KunmingUniversityofScienceandTechnology),
Kunming650093,China;
2.SchoolofMetallurgyandEnvironment,CentralSouthUniversiyt,Changsha410083,China;
3.StateKeyLaboratory ofComplexNonferrousMetalResourcesClearUtilization,Kunming650093,China;
4.YunnanInstituteofProductQualitySupervisionandInspection,Kunming650223,China
◎CentralSouthUniversiytPressandSpringer-VerlagBerlinHeidelberg2014
Abstract:The industrialsilicafumepretreatedbynitricacidat80 。C wasre—used in thiswork.Then.theobtained silica
nanoparticlesweresurfacefunctionalizedbysilanecouplingagents,suchas(3一Mereaptopropy1)rtiethoxysilane(MPTES)and
f3.Amincpropy1) trithoxysilane (APTES).Some ufrther modifications were studied by chloroaceety1 choride and
1,8-Diaminoaphalene foramino modified silica.The surfacefunctionalized silica nanoparticleswerecharacterized by Fourier
transforininfrared(FI-IR1andX.rayphotoelectronspectroscopy(xPS).Thepreparedadsorbentofsurfacefunctionalizedsilica
nanoparticleswim difrerentialfunctiongroupswereinvestigatedintheselectiveadsorptionaboutPb .Cu ,Hg .Cd andZn2
ionsin aqueoussolutions.Theresultsshow thatthef3一Mercaptopropy1)triethoxysilanefunctionalized silicananoparticles
(Si02-MPTES)playanimportantroleintheselectiveadsorptionofCu nadHg ,the(3-Amincpropy1)trithoxysilane(APTES)
functionalized silica nanoparticles (SiO2-APTES)exhibited maximum removalefficiency towardsPb and Hg .the
1。
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