原创力文档《Synthesis and Crystal Structure of 1,4-Bis(benztriazol-1-ylmethyl)-2,3,5,6-tetramethylbenzene》.pdfVIP
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《Synthesis and Crystal Structure of 1,4-Bis(benztriazol-1-ylmethyl)-2,3,5,6-tetramethylbenzene》.pdf
24 卷3 期 结 构 化 学 JIEGOU HUAXUE Vol. 24. No.3
2005. 3 Chinese J. Struct. Chem. 279~282
Synthesis and Crystal Structure of 1,4-Bis-
(benztriazol-1-ylmethyl)-2,3,5,6-tetramethylbenzene
CAI Yue-Penga, b HE Guang-Pinga CAI Yic
a b b
ZHANG Chi SU Cheng-Yong KANG Bei-Sheng
a (Department of Chemistry, South China Normal University, Guangzhou 510631, China)
b (School of Chemistry and Chemical Engineering,
Sun Yet-sen University, Guangzhou 510275, China)
c (School of Pharmacaceutical Sciences, Anhui College
of Traditional Chinese Medicine, Hefei 230038, China)
ABSTRACT The title compound 1,4-bis(benztriazol-1-ylmethyl)-2,4,5,6-trimethylbenzene crys-
tallizes in the monoclinic system, space group Pbca with a = 9.842(5), b = 9.455(5), c = 22.165(12)
3 3 1
Å , V = 2062.6(18) Å , D = 1.277 g/cm , Z = 4, C H N , M = 396.49, m(MoKa) = 0.079 mm
c 24 24 6 r
and F(000) = 840. The structure was refined to R = 0.0662 and wR = 0.1891 for 1163 observed
reflections (I 2s(I)). The title molecule has trans-conformation about the central phenyl ring. The
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