1-苦基硝基咪唑衍生物的合成的研究.pdf

Abstract 硕士论文 Abstract was Inthis of anditsderivatives dissertation，the synthesis1-picrylnitroimidazole ofimidazoleandits in theiodination details，mcluding investigated ofimidazolederivativeswith thenitrationofthederivatiyes condensation chloride，and picryl different was three of synthesizedby iodoimidazoles．1-picryl一4(5)-nitro·5(4)-iodoimidazole ofimidazolederivatives、析mchlorideWas routesandthemechanismofthereaction picryl suchas ratiowhich reactionconditions studied．Meanwhile，the temperature，time，materials werecharacterizedmeansof reactionwere materialsobtained affectthe optimized．The by different to obtain nuclear andinfrared．Threeroutes magnetism，massspectrum showedasfollows： Was 1-picryl一4(5)-nitro一5(4)一iodoimidazole KI／ was raw iodinationwith Thefirst the material，through route：4(5)．nitroimidazole at for4 thecondensationwith chlorideto