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富马酸二甲酯合成的工艺设计
——年产480吨富马酸二甲酯工艺设计
姓名 专业 学号 指导教师 完成日期
目 录
1 设计任务书······················································1
1.1基本数据···················································1
1.2设计内容及要求 ············································1
2 产品简介························································1
2.1富马酸二甲酯的介绍 ········································1
2.2富马酸二甲酯的性质及
2.3富马酸二甲酯的市场分析·····································3
3 生产工艺的选择··················································3
3.1 合成工艺的比较············································3
3.2 本设计采用的工艺··········································4
4 工艺流程设计····················································5
4.1 原料来源及产品规格········································5
4.2 工艺流程简图··············································5
5 物料衡算及热量衡算··············································6
5.1 已知数据··················································6
5.2 顺丁烯二酸与甲醇制备富马酸二甲酯的物料衡算框图············6
5.3 衡算过程··················································6
6 主要设备选型····················································9
6.1 泵的设计及选型············································9
6.2 反应釜的设计及选型········································10
6.3 换热器的选型··············································12
6.4 储罐的选型················································12
6.5 分离设备的选型············································12
7 车间布置设计····················································13
7.1 泵的布置··················································13
7.2 反应釜的布置··············································13
7.3 换热器的布置··············································14
8 环境保护与安全措施··············································14
8.1 环境保护··················································14
8.2 安全措施··················································15
9 设计体会························································16
10 设计一览表·····················································17
11 参考文献··································
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