- 1、本文档共104页,可阅读全部内容。
- 2、原创力文档(book118)网站文档一经付费(服务费),不意味着购买了该文档的版权,仅供个人/单位学习、研究之用,不得用于商业用途,未经授权,严禁复制、发行、汇编、翻译或者网络传播等,侵权必究。
- 3、本站所有内容均由合作方或网友上传,本站不对文档的完整性、权威性及其观点立场正确性做任何保证或承诺!文档内容仅供研究参考,付费前请自行鉴别。如您付费,意味着您自己接受本站规则且自行承担风险,本站不退款、不进行额外附加服务;查看《如何避免下载的几个坑》。如果您已付费下载过本站文档,您可以点击 这里二次下载。
- 4、如文档侵犯商业秘密、侵犯著作权、侵犯人身权等,请点击“版权申诉”(推荐),也可以打举报电话:400-050-0827(电话支持时间:9:00-18:30)。
查看更多
* * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * Constituent analysis of composite materials Different constituents decompose at different and specific temperature; this can be used to identify each constituent and its content. Compositional analysis of copolymers Thermal stability of polymers Anti-oxidization ability A standard constituent analysis has two steps : Temperature raised from 40 to 550 oC in N2 atmosphere. Temperature is reduced to 300 oC, and atmosphere is changed to air with subsequent heating from 300 to 850 oC. Typical TGA trace for a rubber compound In N2 In air TGA curves of ethylene/vinyl acetate copolymers of different compositions in N2 If different segments of copolymer chains have different thermal stabilities, it is possible to quantify them . % vinyl acetate = % weight loss x 1.43 Loss of acetic acid Blending of PS and PVC improves their stabilities. This indicates that some interaction between the components is taking place, leading to mutual stabilization. Prediction based on 50:50 linear addition of the TGA curves of PS and PVC. Experimentally observed TGA curve of 50:50 PS/PVC blend. Part 4 The principle of DMA is basically similar to rheometry. It measures the displacement response of a material to an oscillatory load as a function of temperature: σ = σ0 sin(wt +d) g = g0 sin(wt) E = (σ0 / g0) x sind E = (σ0 / g0) x cosd tand = E/E Single cantilever bending Dual cantilever bending Tension Compression Three point bending Shearing There are different types Geometries for DMA measurements with different configurations, and therefore the modulus measured can be Young’s modulus, shear modulus, or bulk modulus (for compression). E E tand Molecular relaxation processes including glass transition are reflected as a decrease in storage modulus, and peaks in loss modulus and tand during heating. Effect
您可能关注的文档
- PROTEUS仿真开发平台讲课.ppt
- 1-1质点运动的描述浅析.ppt
- PROTEUS仿真平台-ISIS讲课.ppt
- 1-1质点运动描述浅析.ppt
- electricfeild(电场)讲课.ppt
- PROTEUS仿真平台讲课.ppt
- electrochemistry-3讲课.ppt
- ELECTRODENX讲课.ppt
- Proteus基础-3.虚拟仿真工具讲课.ppt
- ElectrostasticField讲课.ppt
- 中国国家标准 GB/T 4797.3-2024环境条件分类 自然环境条件 第3部分:生物.pdf
- GB/T 4797.3-2024环境条件分类 自然环境条件 第3部分:生物.pdf
- 《GB/T 10395.28-2024农业机械 安全 第28部分:移动式谷物螺旋输送机》.pdf
- 中国国家标准 GB/T 10395.28-2024农业机械 安全 第28部分:移动式谷物螺旋输送机.pdf
- GB/T 10395.28-2024农业机械 安全 第28部分:移动式谷物螺旋输送机.pdf
- 高中数学学考复习优化练习20空间点、直线、平面之间的位置关系含答案.docx
- 刘静心 82003005 材加概论结课论文(2).pdf
- 社会实践登记表1.doc
- 刘静心 82003005 材加概论结课论文.docx
- 十三五全面二孩政策解读.ppt
文档评论(0)