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論文修改建議事宜
論文待補實驗
所有微波實驗補上不加催化劑之對照組實驗 Entry Phenol/Naphthol Time (sec) Cat. 3
Yield (%)a Cat. 10
Yield (%)a No cat.
Yield (%)a 1 50 69 84 9 2 50 72 81 11 3 50 78 87 13 4 50 66 71 6 5 50 70 78 8 6 50 71 73 11 7 50 72 80 12
Entry Phenol/Naphthol Time (sec) Cat. 3
Yield (%)a Cat. 10
Yield (%)a No cat.
Yield (%)a 1 50 65 77 2 50 62 71 3 50 60 69 4 50 69 80 5 50 58 66 6 50 70 85
論文修改部分(結果與討論):已完成
P62 IR區域放大圖(νSH)垂直放大
FAB-Mass 之 simulation 與 experiment spectra 比較部份之window 放一樣寬
分子式催化劑X-ray data 之 Cu—O鍵長 (J.T- distortion)現象
XPS (Cu2+ 為何會有Satellite 之原因)
IR spectra
Reference 格式統一
論文修改部分:待完成
英文摘要
緒論前言部分
Zeta-potential (表面電位分析)電位(zeta potential)在膠體化學中,是指膠體粒子上累積的離子所引發的靜電壓;膠體粒子由雙層電子構成,包含固定層和擴散層。一個粒子可以藉由亨利公式(Henrys function)導出電泳的移動率,進而求出其界達電位的值。
Colloidal particles dispersed in a solution are electrically charged due to their ionic characteristics and dipolar attributes.
Each particle dispersed in a solution is surrounded by oppositely charged ions called the fixed layer. Outside the fixed layer, there are varying compositions of ions of opposite polarities, forming a cloud-like area. This area is called the diffuse double layer, and the whole area is electrically neutral.
When a voltage is applied to the solution in which particles are dispersed, particles are attracted to the electrode of the opposite polarity, accompanied by the fixed layer and part of the diffuse double layer, or internal side of the sliding surface.
Dispersed particles Aggregated particles Zeta potential is considered to be the electric potential of this inner area including this conceptualsliding surface. As this electric potential approaches zero, particles tend to aggregate.
The static layer is computed using the following formula (which is embedded in the Zeecom software).
Zeta Potential (Smoluchowski’s Formula)
Zeta potential [mV] Stability behavior of the colloid from 0 to ±5, Rapid coagulation or flocculation from ±10 to ±30 Inc
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