simpledistillation.pptVIP

CHEM 334 Expt 3 Lecture Today:Exp.6: Column Chromatography: The Separation of Ferrocene and Acetyl FerroceneMidterm next Friday in your lab!starting at the beginning of your lab session5 Problem Sets (Total 100 pts.)The exam will include today’s Exp. 6 materialReview/study lab lectures, practice questions, experiments, calculations, graphs.Do sample Midterm questions in ERES file Midterm Rules: Cell phones off and in your pack. Do bring a calculator, but not a computer. No sharing ... Do not leave the room during the exam. No extra note paper; use back of pages if necessary. Please no questions during exam (unless you discover a serious mistake). You can write: if I understand the question this way ... No late exams... A midterm not taken earns the grade F. ? Read questions carefully. Proofread…. Exp.6: Column Chromatography: The Separation of Ferrocene and Acetyl Ferrocene(omit UV/VIS analysis) Exp.6: Column Chromatography: The Separation of Ferrocene and Acetyl Ferrocene Column Chromatographyfollowed by Thin Layer Chromatography (TLC) What is common to all methods of chromatography? ACS Family Science Night Willard Middle School in Berkeley Thursday, Oct. 26, 6:30 – 8:30 pm Next Friday Lab Lecture:Your questions….Remaining Experiments:Exp.8, “Dehydration of 2-Butanol”; GCExp.9, “Separation and Identification of an Unknown Mixture” (3 lab periods); IR, recryst., mp.s and other techniques you learnt this semester * Cyclopentadienyl anion is “aromatic”. What makes it aromatic? In our experiment: Stationary phase: Alumina III Moving phase: Pet. Ether. Later: 50/50 mixture pet. ether/diethyl ether Column Chromatography Setting up the micro-scale Column Chromatography (CC) Procedure: Assemble column. Check flow through the frit by using petroleum ether. Then bring the pet ether volume to a height of ? the column. Slowly add Alumina powder. Goal is to have uniform packing. Do not let the top of the column packing go dry. Add ~1 cm of sand af