2014化工原实验复习提纲(下册)：.docVIP

第一部分 实验基础知识 如何读取实验数据 如何写实验报告 数据处理 一、实验数据的误差分析 1. 真值 　 平均值误差的分类精密度和精确度 实验数据的记数法和有效数字错误认识：小数点后面的数字越多就越正确，或者运算结果保留位数越多越准确。 二、实验数据处理 实验数据中各变量的关系可表示为列表式，图示式和函数式。 分 实验内容 每个实验的原理、操作方法、仪表的使用、实验记录、数据处理、思考题 精馏实验： 物系、实验原理、流程图、数据处理（用公式表示）、思考题 测定指定条件下的全塔效率或等板高度 操作中可调节可控制的量 物料浓度的测定方法 操作步骤，先全回流，再确定一定回流比操作，为什么 实验中出现异常现象（液泛，无回流），如何判断？如何处理？ 进料状态对精馏塔的操作有何影响？确定q线需要测定哪几个量？查取进料液的汽化潜热时定性温度应取何值？ 什么是全回流？全回流操作的标志有哪些？在生产中有什么实际意义？ 其他条件都不变，只改变回流比，对塔性能会产生什么影响？进料板位置是否可以任意选择，它对塔的性能有何影响？为什么酒精蒸馏采用常压操作而不采用加压蒸馏或真空蒸馏？将本塔适当加高，是否可以得到无水酒精？为什么？测定填料塔的流体力学性能测定规定条件下的总吸收系数；分析操作条件对总吸收系数的影响在70—80摄氏度的空气流中干燥，经过相当长的时间，能否得到绝干物料？为什么？通常要获得绝干物料采用什么方法？测定干燥速率曲线有何意义？它对设计干燥器及指导生产有些什么帮助？使用废气循环对干燥作业有什么好处？干燥热敏性物料或易变形、开裂的物料为什么多使用废气循环？怎样调节新鲜空气和废气的　转子流量计。 I signed with the Bank of the qilu Bank loan contract (contract) conventions, and I use scheme, I would request the loans (in words) until I opened personal settlement account with your Bank (account), uses loan for 。 Loan operation, business unit name: account number: loan funds from these personal settlement account into the account of a payment. Loans in accordance with the following payment methods to pay. One, lender trustee payment. Delegate qilu Bank loan funds of the borrower to meet the stipulation of the contract the following borrowers, counterparties, commitment funds, regulatory compliance, legal, and willing to take the pay disputes, loss and other consequences of the delegate. Payee account number Bank name amount purpose II, borrowers own payment methods. Qilu Bank according to the borrowers withdrawal request to loan funds disbursed directly to the borrowers account, and independently by the borrower payments to borrowers who meet the stipulation of the contract transactions. I guarantee to your bank contracts and other prove of material submitted by real and effective. When in accordance with one payment, I agree with the above account with your bank loan funds that are not used for stop payment management,stop paid confirmed book record