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manual- departmentof chemistry home（人工化学家）.doc

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RAIRS CHAMBER MANUAL Rev. January 2005 Introduction 3 Ultra High Vacuum Equipment 3 General 3 Gaskets 3 Removing and Remounting Flange 3 Valves 4 Tubing 4 Manifold 5 Manipulator 5 Power Thermocouple Feedthrough 5 Sample Holder 5 Pressure Gauges 6 Thermocouple 6 Ion gauge 7 Leak Detection 7 Pumping System 7 Overview 7 Mechanical Pumps 7 Turbo Molecular Pumps 8 Cryogenic Pumps 9 IR Chamber 9 Overview 9 Sample Manipulator 10 Dosing of Gases and Vapors 10 How to Vent the Chamber 11 How to Evacuate and Bake Out the Chamber 11 How to Regenerate the Cryopump 12 Opening the Chamber 12 Closing the Chamber and Bake-Out 13 How to clean the Pt(111) surface 13 Sputtering of the Sample with Ar 13 Annealing in Oxygen and Flashing 14 Mass Spectrometer: UTI 100C 14 Engaging the MS 15 Standby Mode 15 Shutting Down 15 Calibration 15 Single Spectra 16 TPD 16 Oscilloscope 16 Temperature Controller 17 How to Heat the Sample 17 How to Cool the Sample 18 Biasing the Sample 18 How to do a RAIRS Experiment 19 Preparation 21 The RAIRS Experiment 21 Getting Started 21 Determine the Sample Position 21 Background Spectrum 22 Sample Spectrum 22 How to do a High-Pressure RAIRS experiment 23 Pressurizing 23 Pumping 23 Maintenance and Occasional Things to do 24 Replacing Thermocouple Wires and Copper Rods Inside the Manipulator 24 Mass Spectrometer Maintenance .24 Take off the Cone of the Mass Spectrometer .24 Put the Cone Back on the Mass Spectrometer .24 Sodium chloride windows .25 Reassembel the Sodium Chloride Windows. .25 Trouble Shooting .26 Sample does not heat. .26 The recorded temperature does not seem to be correct. .26 The MS does not work properly. .26 Things to keep an eye on .27 He Compressor .27 Dry Air Purge .27 Appendix A (Linearized Temperature with Output Voltages .28 Appendix B (Conversion Table for the TC PREAMP OUT for Temperature Below 0oC .28 Appendix C (So