ppt课件-phasechemistryofironoresinters-saimm.pptVIP

Phase development in Iron Sinter Test Pots Cooled with Liquid Nitrogen or Water Authors: T van den Berg and JPR de Villiers University of Pretoria Content Introduction Experimental Procedure Results Conclusions Future work Introduction Sinter properties are dependent on the phase composition Many studies on the final sinter product Evolution of phases during intermediate stages of the process need investigation During the heating stage At maximum temperature – reducing conditions During air cooling - oxidising conditions Quench the test pot to study the reaction sequences and formation of phases in the sinter Mineralogy, microstructure and their evolution can be categorized with the ultimate aim understand the sequence of reactions during sintering Experimental Procedure A normal sinter pot test was started Liquid nitrogen or water was used to quench the reactions Air suction was not stopped Pot was then opened and split through the middle Samples were then collected from the middle section of the pot To eliminate edge effects Experimental Procedure Experimental Procedure Liquid nitrogen cooled pot test: Sinter process was complete from top to bottom Samples taken at numbered locations Sample 8 is the grid layer that consists of sinter Experimental Procedure Water cooled pot test: Sinter process was quenched Samples taken at numbered locations Sample 9 represents the grid layer Experimental Procedure Liquid nitrogen cooled test: 7 samples analysed with XRD Samples 2, 4 and 6 was analysed with SEM and microscope Water cooled test: 8 samples analysed with XRD Future work will include micro analysis of the phases Results Results Results Results Results Results Results Conclusions Liquid nitrogen cooled pot test: It is evident from the time-temperature curves and presence of SFCA at the bottom of the pot that the pot test was not cooled effectively Microscope analyses show that SFCA is associated with magnetite The top and middle parts of the pot contain mai