Research on Kang Fu Yan Granule Technology and Quality Standard.docVIP

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2017-01-23 发布于北京
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Research on Kang Fu Yan Granule Technology and Quality Standard.doc

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Research on Kang Fu Yan Granule Technology and Quality Standard 　　Abstract. This paper aims to confirm the preparation technology of Kang Fu Yan granule and make its quality standard. Orthogonal experimental method is applied to investigate the alcohol extraction volume of rhizoma corydalis (yanhusuo), the volatile oil extraction of rhizoma atractylodis, rhizoma cyperi, angelica and rhizome chuanxiong, the decoction dregs of rhizoma atractylodis and other medicinal materials, and the six-taste water extraction technology of dandelion and other medicinal materials, hence optimizing the technological parameters. The best technological preparation for Kang Fu Yan granule is confirmed in the technological researches. This paper concludes that the method and indexes in this experiment are applicable to the preparation technology of Kang Fu Yan granules. 　　Key words: Kang Fu Yan granules, preparation technology 　　1. Instruments and Reagents 　　Instruments: LC2050 high performance liquid chromatograph, LC2400 ultraviolet detector, N2000 chromatogram workstation 　　Reagents: paeoniflorin reference substance, rhizoma atractylodis reference medicinal materials, angelica reference medicinal materials, rhizome chuanxiong reference medicinal materials,α-cyperone reference substance, and yanhusuo reference medicinal materials; acetonitrile: chromatographic purity; redistilled water (made by ourselves); analytical reagent 　　2. Technological Researches [1] 　　(1) Investigate the alcohol extraction volume of yanhusuo; 　　(2) Investigate the volatile oil and extraction time of rhizoma atractylodis, rhizoma cyperi, and angelica and rhizome chuanxiong by steam distillation; 　　(3) Investigate the decoction dregs after volatile oil extraction, the dandelion six-taste water extraction technology and water volume. 　　2.1 Alcohol Volume Experimental Methods 　　Weigh three pieces of 240g yanhusuo, pour 70% of alcohol based on the designed alcohol volume, extract them respectively at