毕业论文(氯化钠的提纯实验研究).docVIP

纯碱副产物氯化钠的提纯试验研究 摘 要 以公司生产的纯碱副产物氯化钠为研究对象，测定其各组分的含量。探讨在化学沉淀法中沉淀剂的加入量、反应温度、搅拌强度、反应时间等操作条件对除去杂质效果的影响，选出最佳的工艺操作参数，通过正交试验，确定最优组合及判断影响因素的显著水平；探讨在重结晶法中冷却温度、结晶次数等操作条件对除去杂质效果的影响，选出最佳的工艺操作参数，通过正交试验，确定最优组合及判断影响因素的显著水平。实验结果表明，通过化学沉淀法最优组合参数处理后的氯化钠产品其氯化钠含量从90.525%提高到99.515%，水分含量从7.183%下降到0.209%，水不溶物的含量从0.608%下降到0.011%，钙镁总量从1.660%下降到0.1127%，硫酸根离子含量从0.024%下降到0.0151%；而通过重结晶法最优组合参数处理后的氯化钠产品其氯化钠含量从90.525%提高到99.379%，水分含量从7.183%下降到0.271%，水不溶物的含量从0.608%下降到0.015%，钙镁总量从1.660%下降到0.2143%,硫酸根离子含量从0.024%下降到0.0053%。 关键词：蒸氨废液，纯碱副产物，氯化钠，化学沉淀法，重结晶法 SODA ASH BY-PRODUCTS OF SODIUM CHLORIDE PURIFICATION EXPERIMENT RESEARCH Abstract Qinghai Jinfeng Industrial Co., Ltd. production of soda ash by-product sodium chloride for the study, determination of the content of each component.Discusses the chemical precipitation agent in the addition amount reaction temperature stir intensity reaction time to remove impurities operation conditions on the effect of the operation parameters of select the best technology, by orthogonal experiment, to determine the best combination and judgment of effect factors of the significant level;Discusses the heavy crystallization method in The Times of cooling temperature crystallization operating conditions on the effects of the remove impurities, select the best technology operating parameters, by orthogonal experiment, to determine the best combination and judgment of effect factors of the significant level.The experimental results show that,Through the chemical precipitation optimal combination of sodium chloride products processing parameters after the content of sodium chloride increased from 90.525% to 99.515%, moisture content from 7.183% to 0.209%, the content of water insoluble, from 0.608% to 0.011%, total calcium magnesium dropped from 1.660% to 0.1127%, sulfate ion content decreased from 0.024% to 0.0151%；And through the heavy crystallization method optimal combination of sodium chloride products processing parameters after the