standardoperatingprocedures(sops).docVIP

Standard Operating Procedures (SOPs) The 2008 revisions to NR149 contain many new requirements regarding laboratory SOPs. Laboratories must have SOPs (written documents) that detail lab activities and procedures. The code allows a great deal of flexibility in the way the SOPs are designed which leaves it up to the lab to decide. The SOPs may be in electronic form or hard-copy. The code requires that for each method being performed that the laboratory generate a specific analytical SOP. In addition to the analytical SOPs, the code requires that the lab document their procedures for at least 19 specific subjects. These 19 issues can be documented in separate SOPs, grouped together in one SOP, or documented in the Quality Manual as long as they are all covered. Analytical SOPS Analytical SOPs are SOPs that describe exactly how the lab performs the method. There are generally three ways for the lab to create their own analytical SOPs. Option 1: the analytical SOP may consist entirely of the referenced published analytical method. Keep in mind that this option will only work if the lab follows the method exactly (very unlikely). Option 2: the lab may reference a published method and include an addendum that details exactly where the lab deviates from the published method. Note that when this option is used, the addendum must include a date of issue or a date of revision. Generally speaking, this option is considered the most practical approach for small wastewater laboratories. Option 3: the lab may choose to create their own SOP from “scratch” . If this option is chosen the code specifically requires that the SOP includes each of the following elements: 1. Identification of the test method 2. Applicable analytes 3. Applicable matrices 4. Method sensitivity 5. Potential interferences 6. Equipment and analytical instruments 7. Consumable supplies, reagents and standards 8. Sample preservation, storage and hold time 9. Quality control sam