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Coating of hydroxyapatite films on metal substrates by seeded hydrothermal deposition.pdf

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Coating of hydroxyapatite films on metal substrates by seeded hydrothermal deposition

Surface Coatings Technology 205 (2011) 3975–3986 Contents lists available at ScienceDirect Surface Coatings Technology j ourna l homepage: www.e lsev ie / locate /sur fcoatCoating of hydroxyapatite films on metal substrates by seeded hydrothermal deposition Dongxia Liu, Keith Savino, Matthew Z. Yates ? Department of Chemical Engineering and Laboratory for Laser Energetics, University of Rochester, Rochester, NY, 14627, United States? Corresponding author. Tel.: +1 585 273 2335; fax: E-mail address: myates@ (M.Z. Yat 0257-8972/$ – see front matter ? 2011 Elsevier B.V. Al doi:10.1016/j.surfcoat.2011.02.008a b s t r a c ta r t i c l e i n f oArticle history: Received 16 October 2010 Accepted in revised form 6 February 2011 Available online 21 March 2011 Keywords: Crystallization Hydrothermal Hydroxyapatite ElectrochemicalHydroxyapatite (HAP) was successfully coated on various metal substrates by a novel seeded hydrothermal deposition method. A nanoscale HAP seed layer was first formed by a short electrochemical synthesis. The seed layer promotes HAP crystal growth onto the surface during a subsequent hydrothermal crystallization step. The surface morphology andmicrostructure of the HAP coatings can be regulated by varying the reaction temperature, solution pH, calcium-to-phosphorus molar ratio in the starting solution, and hydrothermal deposition time. The new method has advantages over many other reported HAP deposition techniques in that it produces highly crystalline, crack-free, adherent films of uniform thickness. In all the films, the HAP crystals are preferentially oriented with the c-axis normal to the substrate. The as-developed HAP coatings are attractive for applications in the area of bioactive surface modification of metallic implants where the microstructure of the film is advantageous for promoting bone growth.+1 585 273 1348. es). l rights reserved.? 2011 Elsevier B.V. All rights reserved.1. Introduction The crystal structural and compositional simila