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Method for control gas diffusion and bubbles formation in liquid porosimetry.pdf

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Method for control gas diffusion and bubbles formation in liquid porosimetry

a r X i v : p h y s i c s / 0 2 0 7 0 3 0 v 1 [ p h y s i c s .i n s - d e t ] 8 J u l 2 0 0 2 Method for control gas diffusion and bubbles formation in liquid porosimetry Dr. V. Smirichinski? Abstract The main problem in liquid porosimetry, which prevents to see the pore sizes smaller than 2 microns in diameter, is direct gas diffusion flow through a micro-porous mem- brane. This diffusion causes bubbles formation below the membrane and that spoils extrusion (intrusion) data, as one cannot distinguish the volume of extrusion (intru- sion) liquid from the volume of formatted bubbles. The suggested below method cures the problem by creating the liquid flow below the membrane. The flow washes out all of the small bubbles preventing them to grow. That allows using the membrane at higher differential pressures, even higher than minimum bubble point of the membrane, without spoiling data. ?E-mail: smirvi@ 1 I. Description A. Background of the invention A1. Field of the invention The present invention relates to the field of porosimetry, particularly to the liquid (not mercury) extrusion or intrusion porosimeter. In suggested method the porosity is measured by detecting volume of liquid extruded from (or intruded in) the sample by applying step by step increasing (decreasing) gas pressure. The sample is placed on a porous membrane with pore-size less than the pore-size of the sample. A2. Description of the previous art The liquid porosimeter, described by Bernard Miller and Ilya Tyomkin [1], is shown schematically in the Fig. 1. Figure 1: Basic arrangement for liquid porosmetry. It can be used in both liquid extrusion porosimetry (LEP) and liquid intrusion porosime- try (LIP). For the LEP mode a presaturated sample is placed on a micro-porous membrane (membrane is supported by a rigid porous plate). The gas pressure is increased in steps and that causes liquid to extrude from the pores. The largest pores extrude first. The top-loading balance for each pressure ste