Glucose-Assisted One-Pot Synthesis of FeOOH Nanorods.pdf

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Glucose-Assisted One-Pot Synthesis of FeOOH Nanorods.pdf

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Glucose-Assisted One-Pot Synthesis of FeOOH Nanorods

Published: April 22, 2011 r 2011 American Chemical Society 9814 dx.doi.org/10.1021/jp2013754 | J. Phys. Chem. C 2011, 115, 9814–9820 ARTICLE pubs.acs.org/JPCC Glucose-Assisted One-Pot Synthesis of FeOOH Nanorods and Their Transformation to Fe3O4@Carbon Nanorods for Application in Lithium Ion Batteries Ting Zhu, Jun Song Chen, and Xiong Wen (David) Lou* School of Chemical and Biomedical Engineering, Nanyang Technological University, 70 Nanyang Drive, Singapore 637457, Singapore ’ INTRODUCTION In the past decades, rechargeable lithium ion batteries (LIBs) have been widely employed as the power source for various portable electronic devices.15 More recently, they are receiving increasing attention because of the rapid development of electric vehicles that can help to alleviate environment problems. To meet these market demands, intensive efforts have been made by the scientific community to develop new LIBs with more attractive features, including low cost, high energy density, and good cycling performance. Recently, different types of nanos- tructuredmetal oxides have been studied as promising anodes for LIBs because of their high energy density and long cycle life.69 Among them, iron oxides (Fe2O3 and Fe3O4) nanocrystals, which are widely used in MRI contrast agents,10 gas sensor, catalysts, and pigments,11,12 have been extensively investigated as electrode materials for LIBs due to their abundance and envir- onmental benignity. However, the replacement of the commer- cial graphite-based anode materials with these metal oxides is hindered mainly by two issues: large initial irreversible loss and poor capacity retention over extended cycling. It is suggested that carbon coating may be a promising way to improve the cycling performance of nanostructured electrode materials,1316 and there have been a few reports on the fab- rication of carbon-coated iron oxides for LIBs.17,18 It is hypothe- sized that the carbon coating has played dual roles in these electrodes durin