Ti层对316L不锈钢表面TiB2薄膜结合力的影响.pdfVIP

Trans. Nonferrous Met. Soc. China 23(2013) 2957−2961 Improvement of adhesion properties of TiB films on 2 316L stainless steel by Ti interlayer films Mu-jian XIA, Hong-yan DING, Guang-hong ZHOU, Yue ZHANG Jiangsu Provincial Key Laboratory for Interventional Medical Devices, Huaiyin Institute of Technology, Huai’an 223001, China Received 6 September 2012; accepted 17 May 2013 Abstract: The periodic [Ti/TiB ] (n=1, 2, 3) multilayered films were prepared on the substrate of AISI 316L stainless steel by 2 n magnetron sputtering to enhance the adhesion of TiB2 films based on the remarkable mechanical performance of layered films. The influence of periods on microstructure, adhesion and hardness of [Ti/TiB ] multilayered films was studied. X-ray diffraction (XRD) 2 n analysis shows that the monolayer TiB films exhibit (001) preferred orientation, and the preferred orientation of [Ti/TiB ] 2 2 n multilayered films transfers from (001) to (100) with the increase of periods. The cross-sectional morphology of each film displays homogeneity by field emission scanning electron microscopy (FESEM). The hardness of the films measured via nanoindention changes from 20 to 2