Chinese Luohanguo of 9 Determination of organochlorine pesticide residues.docVIP

 PAGE \* MERGEFORMAT 11 Chinese Luohanguo of 9 Determination of organochlorine pesticide residues On: Off Zeming, of down 2, Lianghan Ming, Luo Yu [Abstract] Objective To establish a Chinese Luohanguo of BHC and DDT, PCNB 3 class of organochlorine pesticide residues. Methods reference lt;”China Pharmacopoeiagt;gt; to extract the sample, sulfuric acid sulfonated by gas chromatography Method: The column was CP SIL 24 CB capillary column, initial temperature of 100 , kept 5 min, to 5 / min rise to 220 to maintain 10 min, to 8 / min to 250 to maintain 27 min; 63Ni electron capture detector and external standard content. Results Luohanguo commercial batches of samples were 8 different levels of pesticide residues. Conclusions The method of 9 organochlorine can achieve baseline separation can be used for organochlorine pesticides in Mangosteen residues. [Keywords:] Mangosteen; organochlorine pesticides; gas chromatography (1.Yongkang Pharmaceutical Co.Ltd., Yunfu, Guangdong 527100, China; 2.The Central Laboratory, Guangdong Pharmaceutical College, Guangzhou, Guangdong 510006, China) Abstract: Objective To establish a method for determining 3 kinds of residues of organic chlorine pesticides, including BHC, DDT, PCNB in Siraitiae Fructus.Methods The extracts were prepared according to Chinese Pharmacopoeia and analyzed by gas chromatography with CP SIL 24 CB quartz capillary column and electronic capture eetector (63Ni ECD), and the contents of 9 organic chlorine pesticides were calculated by external standard. Results The organic chlorine pesticides in Siraitiae Fructus were determined and found in all samples collected. Conclusions Separation of the main peaks was achieved. The method can be used to determine organic chlorine pesticides in Siraitiae Fructus. Keywords:: Siraitiae Fructus; organic chlorine pesticides; gas chromatography Mangosteen (Siraitiae Fructus), also known as light fruit turtle, false bitter gourd, gourd plants for the matur