Gynecology Pills TLC.docVIP

 PAGE \* MERGEFORMAT 7 Gynecology Pills TLC [Keywords:] gynecological 9 Abstract: Objective: To study the quality control pills gynecology. Methods: The thin-layer chromatography on gynecological pill cinnamon, Yu Gan, kaempferol for qualitative identification. Results: The three TLC-positive and negative control without interference. Conclusion: The method is reliable and can be used for gynecological pills quality control. Keywords:: gynecological 9; TLC Gynecology pill for a recipe from the Tibetan experience, cinnamon, Yu Gan, wolfberry fruit, pepper, kaempferol, cinnabar, nutmeg, etc. 9 Herbs Honey pill made of water, with Qufeng pain, regulating menstruation blood circulation, heat anti-inflammatory, beauty freckle’s effectiveness: for women, anemia, irregular menstruation, amenorrhea, dysmenorrhea, accessories inflammation, uterine fibroids and so on. I the other side in the cinnamon, Yu Gan, kaempferol had TLC [1,2], now the results reported are as follows. An experimental material Gynecology pills, Yunnan, Chen Xia palm Medical Institute (batch number 040910). Silica gel G, GF254 thin-layer plate, Qingdao Marine Chemical Factory Chupin. Cinnamic aldehyde, gallic acid, p-methoxy cinnamic acid ethyl ester reference substance, the Chinese pharmaceutical and biological products available. The solvents were of analytical grade. 2 Methods and Results 2.1 Identification of cinnamon 2.1.1 Preparation for the test product solution to take this product 20g, research fine, add ethyl ether 50ml ultrasonic treatment 20min, filtration, the filtrate temperature Hui dry residue dissolved in 2ml ethanol added as a solution for the test product. 2.1.2 Preparation of reference substance solution Take cinnamic aldehyde reference substance, add ethanol made from 1μ l/ml solution, as a reference substance solution. 2.1.3 Preparation of negative control solution To take samples of herbs cinnamon missing, according to test products for the solution preparat