Hainan fingerprint of gall wood.docVIP

 PAGE \* MERGEFORMAT 9 Hainan fingerprint of gall wood Of: Li Hailong, Tan Yinfeng, Laiwei Yong, LIU Ming-sheng, Fu is a light, Jun-Qing Zhang [Abstract] HPLC method for the purpose of the establishment of Hainan fingerprint of medicinal wood lamps, wood lamps in Hainan provides quality control of herbal medicine production. Methods using high performance liquid chromatography column was Diamonsil TM C18 (250 mm 4.6 mm, 5 m, the detection wavelength was 227 nm, mobile phase of methanol -0.10% phosphoric acid solution, gradient elution. Results fingerprint Hainan gall wood, a total of peak relative retention time and relative peak area precision, repeatedly and stability of the RSD were less than 3%, in line with the requirements. Conclusions The fingerprints can be used to Hainan gall wood quality control of medicines. [Keywords:] Hainan gall wood, high performance liquid chromatography, fingerprinting, quality control Abstract: ObjectiveTo establish the Fingerprint Chromatography of Hainan Nauclea officinalis by HPLC and provide the method for quality control of Hainan Nauclea officinalis.MethodsAn HPLC method with the Diamonsil TMC18 column (250 mm 4.6 mm, 5m) and a mixture of methanol-0.10% phosphoric acid solution (dual gradient elution) as the mobile phase was used. The dectection wavelength was set at 227nm. ResultsHPLC fingerprint chromatography of 10 batches of samples was established. The results showed that this method had a good repeatability and the 8 common peaks had an exclusive properties. ConclusionThe fingerprint established can be used for quality control of Hainan Naucleae officinalis. Keywords:: Hainan Naucleae officinalis; HPLC; Fingerprint; Quality control Gall wood tree species madder Ke Wu Wu Tan Tan Naudea oftcinalis Pierrc ex Pitard, dry stem and root, with detoxification, swelling and pain and other effects. Bile in China has been using wood wood injection and bile extract tablets, treatment Leptospira and upper