High Performance Liquid Chromatography pharyngitis content of the film harpagoside.docVIP

 PAGE \* MERGEFORMAT 9 High Performance Liquid Chromatography pharyngitis content of the film harpagoside [Abstract] Objective: To establish a method for determination of tablets pharyngitis. Methods: The high-performance liquid chromatography. Column: Agilent TC-C18 (250mm * 4.6mm, 5μ m), Mobile phase: acetonitrile -1% acetic acid solution of a linear gradient elution, flow rate: 1.0ml * min-1, detection wavelength: 278nm, column temperature: 40 ℃ . Results: harpagoside in the 1.0 ~ 50.0μ g * ml-1 range of a good linear relationship (r = 0.9997); The average recovery was 98.1%, RSD = 1.9% (n = 6). Conclusion: This method is simple, accurate and reliable, suitable for pharyngitis film quality control. [Keywords:] high-performance liquid chromatography pharyngitis film harpagoside Determination Determination of Harpagoside content in Yanyan tablets by HPLC [Abstract] Objective: To set up a method for quality control of Yanyan tablets. METHOD HPLC method was developed to quantitative determination. Agilent TC-C18 (250mm * 4.6mm, 5μ m). The mobilic phase was acetonitrile-1% acetic acid solution in linear gradient elution.The column temperature was 40 ℃ , the wavelength for detection was 278nm, flow rate was 1.0ml * min-1. RESULTS The Harpagoside average of recovery rate was 98.1%, and RSD was 1.9% (n = 6) . CONCLUSION The method is simple, accurate and suitable for its assaying. [Keywords:] HPLC; Yanyan Tablets; Harpagoside; Determination Pharyngitis piece for the ‘Ministry of Health, Drug Standards’ second book (TCD Narikata preparation) containing relevant varieties, from the Scrophulariaceae, 100 (system), days of winter, Cortex Moutan, Ophiopogon japonicus, Coltsfoot Flower (system), wood butterfly, to yellow, Banlangen, fruit, oneself, peppermint oil composed of 12 Chinese herbal medicines, with Yin lungs, Qingrejiedu Qing Li throat, itching of the antitussive effect. Clinical use of chronic pharyngitis caused by throat, pharyngeal itching, irrita