Night Capsules Quality Standards.doc

 PAGE \* MERGEFORMAT 11 Night Capsules Quality Standards Author: Ding Li Ying Zhou Cai Chun Dragon Asia, [Abstract] Objective: To study and formulate the Night Capsules quality standards. Methods: The thin-layer chromatography and HPLC method. RESULTS: Emodin in 5-25μ /ml showed good linear relationship within the regression equation was y = 39931.1A-22660.4, r = 0.9998. Each and Shouwu vine to emodin terms, shall not be less than 0.05mg. Conclusion: The sample repeatability and precision of the inspection proved this Act stable, reliable, fast, accurate and can be product-oriented quality control methods. [Keywords:] Night Capsules Emodin TLC HPLC; assay Night Capsules for the 2005 edition of ‘Chinese Pharmacopoeia’ collected a set of ‘Night-ning syrup’ and retrofit preparation; mainly by Albizia, Shouwu rattan, drugs such as the composition of Ganoderma lucidum. The main ingredients of Albizia Fang, Ganoderma lucidum, Shouwu rattan and other varying degrees of calm and soothe the nerves of the role; in the development of the product quality standards, we used thin-layer chromatography identification of Albizia, respectively, Ganoderma lucidum, Shouwu vine, licorice 4 taste herbs, and at the same time use the content of emodin as the product control targets, because in this product emodin for Chen Shou Wu Teng drug detection methods and components unique to mature, and reliable; so we opted for emodin-based products The determination of control targets. 1 instruments and reagents 1.1 The instrument of Shimadzu LC  10ATvp-based high-performance liquid chromatography (Shimadzu Corporation), RE  52C rotary evaporator (Shanghai Qingpu Huxi Instrument Factory), FQC  100 Ultrasonic Cleaning Machine (Wuxi Funide Electronic company frequency 40KHZ), SC202  1 Type Electric Ovens (Tong Tong Zhou Shanghai Pharmaceutical Machinery Equipment Factory), FA1004-type one hundred thousandth electronic balance (Shanghai Precision Scientific Instrument Co., Ltd.),