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Quality Standard compound of Sophora_0
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Quality Standard compound of Sophora
[Abstract] Objective To develop a compound for the quality standards of bitter beans. Methods of thin layer chromatography, respectively, in compound hawthorn, cassia, qualitative identification alopecuroides by HPLC in the main drug of Semen for chrysophanol content. Results thin layer chromatography, sample solution and the reference drug or reference substance in the corresponding position in the same color of the spots appear on the negative non-interference, high performance liquid chromatography, chrysophanol 0.028 4 ~ 0.908 8 μg range showed a good linear relationship, r = 0.999 7 (n = 6), the average recovery was 99.97%. Conclusion This TLC method used in specific, high performance liquid chromatography, high precision, repeat , and can be used for the preparation of quality control.
[Keywords:] compound alopecuroides capsules, TLC, chrysophanol, high performance liquid chromatography, quality standards
Abstract: Objective To establish the quality standard for Complex Prescription Kudouzi Capsules. Methods TLC was employed to identify Crataegus pinnatifida Bge., Cassia obtusifolia L. and sophora alopecuroides L.. The content of chrysophanol in Cassia obtusifolia L. was determined by HPLC. Results Spots obtained from the test solutions had the same color in reference solution and medical material in the same location, and the blank solution had no interference. The linear range of chrysophanol was 0.028 4 ~ 0.908 8 μg, r = 0.999 7 (n = 6 ), and the average recovery was 99.97%. Conclusion The characteristic of identification by TLC was highly specific, HPLC is accurate and reproducible, and they can be used effectively for the quality control of Complex Prescription Kudouzi Capsules.
Keywords:: Complex Prescription Kudouzi Capsules, TLC, chrysophanol, HPLC, quality standard
Sophora compound capsule is used for many years on the basis of clinical prescription, after the crushing
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