Quality Standard Zhibai Dihuang Wan.doc

 PAGE \* MERGEFORMAT 3 Quality Standard Zhibai Dihuang Wan [Abstract] Objective To establish quality standards Zhibai Dihuang Wan. Methods used in the TLC method Zhibai Dihuang Wan dogwoodResults TLC specific. Loganin good linear relationshipConclusion The method is simple[Keywords:] Zhibai Dihuang Wan; thin layer chromatography; high performance liquid chromatography; quality standards Zhibai Dihuang Wan (Pill) is a dogwooddry mouth and sore throatZhibai Dihuang Wan (Pill) received drug standards set out in the Ministry of HealthFang dogwood with liver and kidney tonicIn order to further improve the variety and quality standardsAre reported below. An instrument and reagent 1.1 Reagents and herbs TLC silica gel G110742-200516)Pharmaceutical and Biological Products provided negative samples provided by the manufacturer. Methanol1.2 Instrument Shimadzu LC-2010C HPLC system (Shimadzu Corporation; include: vacuum degasser); FA2104 electronic balance (Shanghai Precision Scientific Instrument Co.2 Methods and Results 2.1 TLC 2.1.1 moutan take the product powder 15 gIn another paeonol reference substanceThin layer chromatography [5] testagentTest products for chromatography2.1.2 Cork take the product powder 1 gIn another berberine reference substanceThin layer chromatography [5] testagentTest products for chromatography2.1.3 dogwood take the product powder 5 gIn another ursolic acid reference substanceThin layer chromatography [5] testas the agentTest products for chromatography2.1.4 Anemarrhena take the product powder 30 gfiltrate was concentrated to 20 mlallows the dissolvedSmilax Lease sapogenin an alternative reference substanceThin layer chromatography [5] test8% ethanol solution of vanillin and sulfuric acid (7-10) of the mixture (0.5:5)Test products for chromatography2.2 Determination 2.2.1 Preparation of reference substance solution Weigh Loganin precision reference standardLinks to free paper download 2.2.2 Preparation of the test so