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Electrochemical Determination of Pentachlorophenol in Water on a Multi-Wall Carbon Nanotubes-Epoxy Composite Electrode.doc

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Electrochemical Determination of Pentachlorophenol in Water on a Multi-Wall Carbon Nanotubes-Epoxy Composite Electrode

Sensors 2012, 12, 7033-7046; doi:10.3390/s120607033 OPEN ACCESS sensors ISSN 1424-8220 /journal/sensors Article Electrochemical Determination of Pentachlorophenol in Water on a Multi-Wall Carbon Nanotubes-Epoxy Composite Electrode Adriana Remes 1, Aniela Pop 1, Florica Manea 1,*, Anamaria Baciu 1, Stephen J. Picken 2 and Joop Schoonman 3 1 Department of Applied Chemistry and Engineering of Inorganic Compounds and Environment, “Politehnica” University of Timisoara, Victoriei Sqr., No. 2, Timisoara 300006, Romania; E-Mails: remes_adriana@ (A.R.); aniela.pop@chim.upt.ro (A.P.); anamaria.baciu@chim.upt.ro (A.B.) 2 NanoStructured Materials, Department of Chemical Engineering, Delft University of Technology, Julianalaan 136, 2628BL Delft, The Netherlands; E-Mail: S.J.Picken@tudelft.nl 3 Materials for Energy Conversion and Storage, Department of Chemical Engineering, Delft University of Technology, Julianalaan 136, 2628BL Delft, The Netherlands; E-Mail: J.Schoonman@tudelft.nl * Author to whom correspondence should be addressed; E-Mail: florica.manea@chim.upt.ro; Tel.: +40-256-403-070; Fax: +40-256-403-069. Received: 30 March 2012; in revised form: 18 April 2012 / Accepted: 26 April 2012 / Published: 25 May 2012 Abstract: The aim of this study was the preparation, characterization, and application of a multi-wall carbon nanotubes-epoxy composite electrode (MWCNT-EP) with 25%, wt. MWCNTs loading for the voltammetric/amperometric determination of pentachlorophenol (PCP) in aqueous solutions. The structural and morphological aspects of the MWCNT-EP composite electrode were examined by scanning electron microscopy. The electrical properties were characterized by direct-current conductivity measurements in relation with the percolation threshold. The electrochemical behavior of PCP at the MWCNT-EP composite electrode was investigated using cyclic voltammetry in 0.1 M Na2SO4 supporting electrolyte in order to estab