氧化锆陶瓷px-242A低温老化性能初步分析.pdfVIP

问院院学研究 2011 年 7 月第 27 卷第 7 期 555 氧化铅陶瓷 px-242A 低温老化性能初步分析 *~直黄慧玉宇华张富强· (上海交通大学民学院附属第九人民原陇·口R盘阪学院口舷修复科 ·上海市口腔医学重点实验室 上海 20001 1) [摘要] 园的:初步分析一种 3 靡尔纪稳定的纳米氯化镣陶甏(TZ-PX一242A) 的低温老化性能。方法:将烧然后 的氧化错试件隧机分成4 组，在高温高压灭商锅!IB挂行循环热处理，处理条件为在 134 c、0.2 MPa 下，进行。 h.l h.3 h.5 h 不同时间的低激1;化实骏。测1量低描画老化实验前后的二三点弯曲强度，并ffl XRD 分析试件司提醒自单斜榕的 比例.结S怪:随着低插i!.;f化时间的延伏，试件表6西单斜栩含t量增加.三点弯曲强If~追逐渐下降趋势.低淄;/Æ化处毯 5 h 后强度仍高于 1100 MPa。结论:本实验用氧化锯陶擎的低温老化性能具备Bt效依赖性，低温恶化对-点弯曲 强度x:明显影响. [关键诩]掏钱氧化错机械做能低#董老化 [中阁分类哥哥] 民783.1 [文献标识码] A [交意缩得] 1671一7651(2011)07…0555-03 Erf，时恼。r Low Tempera阳reDψadatloD OD Zlrω恨ia Ceramic( px …242A). JIANG H时• HUANG Hui. Wang Yu- h时• et al. Department 01 Prosthodontics. The Nínth People s Hospítal. College 01 Stomatology. Shanghaí Jiao γong University School 01 Medícine. Shanghaí Key Laboratory 01 Stomatology. Shanghaí 200011 [Abstract] ObJective: To investigate the influence of in vitro low-temperature degradation(LTD) of a 3% Y ,O , stabilized tetragonal zirconia polycrystals. Metb制15: Specimens were divided into 4 groups and subjected to an accel- 盯ated aging test carried out ín an autocJ ave ín 盯制m at 134C, 0. 2 MPa.!or O, I , 3.and 5 h. X-ray diffractíon (XRD was used 10 identify crystal phase前 and relatíve content of monoclinic phase was calculated. And bendíng strengh w拙 tested before and after aging. R，倒nlts ， The relative content of monoclinic phase was increasing with the prolonged aging time. And the flexural strength was above 1100MPa after 5 hours of aging. ConclUllÎon I The results suggest thst LTD of the zirconia ceramic is time dependent and the bending strength after aging is not obvious. [Key words] Ceramic Zirconia Flexural strength Low temperature degradation