气相色谱快速固体进样技术及氦放电光离子化检测器的研发.pdfVIP

A b str a C t A t Present，th e tren d s in develoPm ent of gas ehrom atograp h y (G C ) are m ain ly goin g to w ard s tw o a sP ects : q u iek d e te etio n an d fie ld an a ly sis b y P o rtab le G C . B a se d o n th e se ten d en e ie s，tw o re lated re seareh w o rk s for G C w ere d ev e lo P e d a n d su m m ar iz e d in th is th e sis. In th e first w o rk ，a d ire et so lid sam P le in tro d u etio n m eth o d for G C w a s d ev e lo P ed to d e tee t P e stic id e resid u e in ero P s. T h e P ro P o se d m eth o d w a s q u ick an d sim P le sin e e th ere w a s n o n e e d for an y sam P le P re 一treatm en t d u rin g th e a n a ly sis. T h a lik s to th e se a d v an ta g e s th is m eth o d w a s su itab le for q u iek d eteetio n for P e stie id e re sid u e in cro P s an d larg e一sea le sereen in g o f sam P le ，Wh ieh enh an e ed th e e ffi c ien ey for th e d e tectio n . In an o th er w o rk ，a h elium diseharge Photo一ion ization deteetor (H e一P ID ) w as dev eloP ed to w ork as a G C d eteeto r. H e一P ID P o sse sse s a d v an tag e s lik e sim P le stru etu re ，m in iatux iz atio n an d h ig h sen sitiv ity . B e sid e s，H e 一P ID 15 a u n iv ersa l d eteeto r 、v h ieh 15 e ap a b le o f d eteetin g m o st o f th e v o latile o rg an ie eo m P o u n d s. T h ere fore ，H e 一P ID 15 a P o ten tia l d ete eto r for P o rtab le G C D iseu ssio n s ab o u t th e ab o v e re se areh w o rk s are su m m ariz e d in th e fo llo w in g eh aP ters : In C h apter O ne，the baek groun d an d Purpo se for th is researeh w ere dem on strated .Q u iek d etectio n a n d fie ld an a ly sis b y P o rtab le G C h a s b e en th e tren d s in d eV e lo P m en t o f G C . R e