镍纳米纤维及镍纳米颗粒的制备和性能表征.pdfVIP

Preparation and Characterization of Nickel Nanofibers and Nanoparticles ABSTRACT During the past decade, Ni nanofibers, as a novel magnetic material, have been attracted intensive attention due to their potential applications in fields such as sensors, biomagnetic devices and hydrogen fuel cell . There are many methods to prepared nanofibers, such as template method, self -assembly method and so on. In recent years, electrospinning method has been used to prepare some 1-D nanostructure nanofibers . Compared with the conventional methods mentioned above, electrospinning is a simple and effective method to produce continuous nanofibers with uniform diameters . However, synthesis of nickel nanofibers by electrospinning has been seldom reported. In this paper Ni nanofibers were successfully obtained by electrospinning using the raw materials of Ni (NO ) and PVA. In order to compare the properties of 3 2 Ni nanofibers, Nickel nanoparticles were obtained by Sol -Gel method. These nanomaterials were characterized by XRD, FTIR, TG-DSC, SEM, TEM, VSM and laser particle analyzer. PVA/Ni (NO ) composite nanofibers were prepared successfully by 3 2 electrospinning. The parameters to control the fiber’s diameter and continuity in the electrospinning process were also studied , and the PVA concentration of 13 wt % , applied voltage of 20kV and collector distance of 15cm were used as the optimal parameters to prepare composite nanofibers and PVA/Ni (NO ) composite