大型铸锻件产品中氢的检测与控制.pdfVIP

学兔兔 大型铸锻件产品中氢的检测与控制 刘金祥，岳 军，王晓光 (二重集团(德阳)重型装备股份有限公司检测中心，四川 德阳618013) 摘要：简述了大型钢铸锻件中氢的来源，分析了样品的采集、加工、清洗、测定对氢分析结果 的影响，解决了生产中氢分析结果波动过大的问题，提出科学合理的氢分析结果评价标准和异 常氢结果的解决方案。试验表明：定氢试样适合用四氯化碳或丙酮进行超声清洗；严格控制取 样和制样过程，合理选择分析参数，保持仪器处于稳定状态并规范操作，可以实现氢含量精确 分析，得到准确的氢分析结果。 关键词：大型铸锻件；氢含量；化学分析 中图分类号：TG1 15．3 1 文献标识码：A 文章编号：1673-3320(2015)03-0023-04 Detection and Control of Hydrogen Content in Large Castings and Forgings LIU Jinxiang，YUE Jun，WANG Xiaoguang (DetectingTesting Center of China E~hong Group(Deyang)Heavy Industries Co．，Ltd Deyang 61 801 3，Sichuan，China) Abstract：The source of hydrogen in large castings and forgings were discussed briefly,and the effects of collection，processing，cleaning and detecting for samples on the analysis results of hydrogen content were analyzed．The problem on too big changes of analysis results for hydrogen content was solved in production．The evaluation of the scientific and reasonable analysis results for hydrogen content and the solutions on abnormal results of hydrogen were put forward．The experiment shows that the samples are suitable for ultrasonic cleaning with carbon tetrachloride or acetone．By strict control of sampling and preparation process，reasonable selection of analysis parameters，keeping the instrument in a stable state and regulating the operation，the precise analysis of hydrogen content can be realized to get accurate hydrogen analysis results． Key words：large castings and forgings；hydrogen content；chemical analysis 核电是清洁高效的能源，国内外对核安全问 材料的性能影响极大，甚至导致大型铸锻件白点和 题都非常重视。作为核电主设备的关键部件—— 开裂，引发重大的事故和损伤。为减轻钢中氢的危 核电大型锻件，对核电压力容器的长寿命、安全 害，需要采用特殊的工艺进行去氢处理。由于部分 性的作用至关重要。由于使用条件恶劣和安全性