高效液相色谱-电喷雾质谱分析牛肉组织中的氟喹诺酮 5989-0596CHCN.pdfVIP

!# ! !#$%() ! Ralph Hindle !#$%()*+,-./01 Access Analytical Lab #3. 2616 - 16 Street N. E. !#$%$()*+,-./ ! Calgary, Alberta T2E 7J8 !# !#$ !%#()* Canada !#$Annex 1 (EEC) No. 2377/90 Chin-Kai Meng !#$%()*+, (MRL) ( Agilent Technologies, Inc. 2850 Centerville Road !#$%) 200 µg/kg ! Wilmington, DE 19808-1610 !#$% (MRL) 300 µg/kg ! USA !# !# (MRL) 200 µg/kg [1] !#$%()*+,-./01 !#$%()*+,-./01234%567 !#$%#()*+,- ! !#$%() ! ! !# !#$%()*+,- !# !(HPLC-ESI-MS) !#$%( !#$% !#$%((SPE) µµ !#$%()*+,-./01 !#$% 33 µg/kg (ppb) !#$% µµ µµ !#SPE ! !#$- !73%-96% !8-19 µg/kg !#$ µµ µµ [2]Chen Schneider[3] !#$% !#$%200 µg/kg !#$% µµ ! !#2002/657/EC !#$%( !#$% !#$%()* !#$% !#$% !#$2002/657/EC 96/23 ! !#$%100 µL 98 !#$100 mL Annex 1 B !HPLC- !#[4] ! !#$%B (MS) ! (SIM) !#$% !()* ! !#$%(100 µL 98 !#$ HPLC/MS !#$%()*+,- 100 mL !# !#$%()*+,-. !33 µg/ kg ! #$ !#$2002/657/EC Ultra-Turrax T25 !50 mL !#$% !# 13 mm !#(PEDF) !(0.2 µm) VWR ! !#$(IS) !#$% !#$%()*+, !#$ !#$% !#$%()*+, -20% +10% !# 100 ng/mL (ppm) !1 !(CV) (%) !#$100 µg/kg CV !# 4 ! !#