BiFeO3的水热合成、表征及光催化性能研究.pdfVIP

• 35 • BiFe03 的水热合成、表征及光催化性能研究/谢会东等 BiFe03 的水热合成、表征及光催化性能研究祷 谢会东，贡彩霞，靳莉，王康康，江元汝，王晓昌 (西安建筑科技大学理学院，西安 710055) 摘要 以 Bi(NÜ:J h • 5H 0和 Fe(N臼)3 .9H O 为原料，KOH 为矿化剂，聚乙二醇 6000 为分散剂，水热合 z 2 成了单相 BiFeα 粉体，利用 X射线衍射、扫描电镜优化了水热合成条件，利用振动样品磁强计测定了 BiFeÜ:J的磁滞 回线，并对产物进行了光催化降解甲基橙性能的研究。结果表明，200C 条件下反应 6h 制备的 BiFe仇粉体显顺磁 性，紫外光照射他对甲基橙的降解率可达 90%。 关键词 水热合成 BiFEÛ3表征光催化 中图分类号:臼1 1. 4 文献标识码:A Hydrothermal Synthesis , Characterization and Photocatalytic Properties of BiFe03 XIE Huidong , JIA Caixia , JIN Li , WANG Kangkang , JIANG Yuanru , WANG Xiaochang (School of Science , Xi an University of Architecture and Technology , Xi an 710055) Abstract Single phase of BiFeÜ:J powder has been synthesized by the hydrothermal method , using Bi(Nα)3 • 5H O and Fe(NÜ:J h • 9H 0 as raw materials , KOH as mineralizer , polyethylene glycol 6000 as dispersant. The hy- z 2 drotherm且1 synthesis ∞nditions were optimized by X-ray powder diffraction and scanning electron microscope. The m且gnetic hysteresis loop of BiFeÜ:J was measured by vibrating-sample magnetomete瓦 Experiment results show that BiFeÜ:J powders prepared at 200C for 6h are paramagnetic with high photocatalytic properties , and the degradation ef- ficiency of methyl orange is near 90 % under UV light irradiation for 4h. Key words hydrothermal synthesis , BiFe(马， characterization , photocatalysis 用X 射线衍射(XRÐ) 、扫描电镜(SEM)研究和优化了水热 0 冒|