两种预还原剂对化妆品中砷测定结果的比较.pdfVIP

现代预防医学2∞8 年第 35 卷第 3 期 Modem Prcventive Medicine 、 2∞8. Vo1.35. NO.3 541 文章编号: 1 ∞3-8507(2∞8 )-03-0541-02 中图分类号: R995 文献标识码:A [实验技术及其应用} 两种预还原剂对化妆品中呻测定结果的比较 刁春霞，刘泼，杨华梅 摘要: [目的]比较两种样品预还原剂对化妆品中叶含量测定结果的区别。[方法]利用氢化物原子荧光光度 法测定化妆品中呻，分别用硫服和硫服-抗坏血酸作为样品预还原剂，采用加标回收试验，比较两种预还原剂对测定结 / 呆的影响。[结果]两种预还原剂对测定化妆品中碑的结果、回收率和精密度无显著差别。[结论]测定化妆品中 ? 神时可以用硫服替代硫腺-抗坏血酸作为样品预还原剂。 关键词:原子荧光光谱法:化妆品;碎:预还原剂 ,., / /; COMPARISON OF TWO KINDS OF PRE-REDUCING AGENTS FOR DETERMINATION AR- SENIC 剧 COSMETICS DIAO Chun-xïa, L/U Bo , YANG Hua-mei. (Taizhou Centerfor Diseω Con­ trol and Prevention , Taizhou 2253∞， China) Abstract: [ Objective] Compared with two kinds of pre-reducing agentsωdetermine amenic in cosmetics. [Methods ] 白llOW回回d thiourea-ascorbic acidω 由e pre-reducing agents wer哩 appliedωdetermine 出e contents of ar悦目c in cosmetics by the atomic fluorescence spectrometIγmethod. Compared and analyzed the affection of determination resul恼。If two pre-reducing agents by the recovery t回ι[Results] There were no significant differences in resul钮， recoveri西皿d precisions of two kinds of pre-reducing agents. [Conclusion] Determination on arsenic in cosmetics 饵nuse 也io山ea to take place of thiourea-幽∞rbic acid as a pre-reducing agent. Key words: Atomic fluorescence spectrometry; Cosmeti臼; Arsenic; Pre-reducing agent r fH 砰及碑化合物有较大的毒性，长期使用含碑高的化妆品可 nglml) :准确吸取一定量的碑标准贮备掖用 5%硝酸溶被逐步 造成皮