铬铁合金(国外英文资料).docVIP

铬铁合金(国外英文资料) Q/SJFC. J08-015.4-2008 Dioxin method for determination of nickel 1 scope In this paper, the calculation of the method, reagent material, instrument and equipment, analysis step, and analysis results of the method of determination of nickel content in the method of the method of determination of the nickel content in the method of measuring the nickel content is given by this standard. This standard applies to the determination of nickel in micro, medium and low carbon ferrochrome, measuring range (quality score) : 0.8%. 2 methods feed Sample after acid dissolution, then through the perchlorate smoke, in the presence of oxidant, alkaline medium, nickel was oxidized into four price, and then and butyl ketone oxime complexation into a kind of soluble complexes, wine red in spectrophotometer at 480 nm wavelength photometric measurement. Three reagents 3.1 hydrochloric acid (rho 1.19 g/mL) 3.2 perchloric acid (rho 1.67 g/mL) 3.3 hydrochloric acid (1 + 1) 3.4 nitrate (1 + 1) Sodium 3.5 (250g/L) 3.6 hydroxide solution (100g/L) Potassium 3.7 potassium sodium salt solution (250g/L) 3.8 persulfate solution (250g/L) 3.9 ethanol (no water) 3.10 diketone of ethanol solution (10g/L) 3.11 iron standard solution: according to 0.2000 g of pure iron powder in 350 ml beaker, with 30 ml of hydrochloric acid (3.3), and dissolution of heating, cooling to room temperature, out into a 200 ml volumetric flask and diluted to scale, blending. This solution contains 1mg of iron. 3.12 standard aqueous solution 3.12.1 called 0.2000 g of pure nickel powder, put in 250 ml beaker, add 20 ml nitric acid (3.4) and the above-mentioned dish, cool to room temperature after heating to dissolve, out into a 1000 ml volumetric flask and diluted to scale, blending. This solution is 1mL containing 200ug nickel. Remove the 10.00 mL nickel standard solution (3.12.1), in 200mL volumetric flask, dilute to the scale and mix well. This solution is 1mL containing 10ug nickel. 4 samples Q/SJFC. J08-015.