丙烯腈_衣康酸铵共聚竞聚率的测定及共聚组成的控制_张寿春.pdfVIP

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丙烯腈_衣康酸铵共聚竞聚率的测定及共聚组成的控制_张寿春.pdf

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31 4 Vol.31 No.4 2006 8 Hi-Tech Fiber Application Aug. 2006 030001 - PAN γ γ Fineman-Ross AN - AIA AN 1.30 AIA 0.59 AN PAN AIA PAN TQ325.8 A 1007-9815 2006 04-0025-05 Measurement of Activity Ratio in AN-AIA Polymerization and Co-monomer Content Control ZHANG Shou-chun, WEN Yue-fang, YANG Yong-gang (Key Laboratory of Carbon Materials, Institute of Coal Chemistry, CAS, Taiyuan 030001 China) Abstract: Activity ratio of acrylonitrile (AN)-ammonium itaconic acid (AIA) copolymerization system and the changes of AIA content in two methods of comnonomer adding were studied in this paper. The activity ratio of AN and AIA measured by Fineman-Ross method was 1.30 ( γ AN) and 0.59 ( γ AIA), respectively, which revealed that the AN-AIA copolymerization was a non-ideal and unstable system. Element analysis and thermogravimetry showed that the change extent of average AIA content was effectively controlled as acrylonitrile was supplemented stage by stage, and the thermal stability of resins prepared by acrylonitrile supplementing method was better than that of resins synthesized without acrylonitrile supplementing. Key words: polyacrylonitrile; activity ratio; thermal stability