实验2 中药制剂的理的化定性鉴别 合并.pptVIP

中药制剂理化定性鉴别 Evaluation only. Created with Aspose.Slides for .NET 3.5 Client Profile 5.2.0.0. Copyright 2004-2011 Aspose Pty Ltd. 一,目的要求 1,熟悉中成药分析的理化定性方法.  Evaluation only. Created with Aspose.Slides for .NET 3.5 Client Profile 5.2.0.0. Copyright 2004-2011 Aspose Pty Ltd. 二．实验原理 通过理化方法观察中药制剂中处方组成 Evaluation only. Created with Aspose.Slides for .NET 3.5 Client Profile 5.2.0.0. Copyright 2004-2011 Aspose Pty Ltd. 三,实验内容 1,大黄流浸膏中大黄升华的鉴别:(1)鉴别方法①取本品1mL，置于坩埚中，坩埚上覆盖载破片，置于石棉网上加热，至载玻片上出现升华物后，放冷，观察，之后加氢氧化钠试液，结晶溶解，观察颜色。  Evaluation only. Created with Aspose.Slides for .NET 3.5 Client Profile 5.2.0.0. Copyright 2004-2011 Aspose Pty Ltd. Evaluation only. Created with Aspose.Slides for .NET 3.5 Client Profile 5.2.0.0. Copyright 2004-2011 Aspose Pty Ltd. 2.牛黄解毒片 ②取本品6片(包衣者除去包衣),研细,加乙醇10ml,温热10分钟（60摄氏度）,滤过,取滤液5ml,加镁粉少量与盐酸0.5ml,加热（水浴）,观察颜色; 另取滤液4ml,加氢氧化钠试液,观察颜色,再加30%过氧化氢溶液,红色不消失,加酸成酸性时,观察颜色变化. Evaluation only. Created with Aspose.Slides for .NET 3.5 Client Profile 5.2.0.0. Copyright 2004-2011 Aspose Pty Ltd. 3,穿心莲片 (1)本品为穿心莲浸膏片(2)鉴别方法①取本品5片,除去包衣,研细,加乙醇10ml,置水浴中加热至沸,加活性炭0.5g,搅拌,滤过. 取滤液1ml,加二硝基苯甲酸试液与乙醇制氢氧化钾试液的等容混合溶液2滴,摇匀,观察颜色; 另取滤液1ml,加碱性三硝基苯酚试液3～5滴,观察颜色. Evaluation only. Created with Aspose.Slides for .NET 3.5 Client Profile 5.2.0.0. Copyright 2004-2011 Aspose Pty Ltd. 4,银黄口服液 (1)本品为金银花提取物,黄芩提取物经加工制成的口服液.(2)鉴别方法①取本品1ml,加5%硝酸钠溶液与10%硝酸铝溶液各0.3ml,生成的有颜色沉淀,再加5%氢氧化钠溶液使成碱性,沉淀即溶解,观察溶液.②取本品0.1ml,加水10ml,摇匀,取溶液2ml,加5%二氯氧化锆溶液1～2滴,观察颜色,再加盐酸1～2滴,观察变化. Evaluation only. Created with Aspose.Slides for .NET 3.5 Client Profile 5.2.0.0. Copyright 2004-2011 Aspose Pty Ltd. 5,板蓝根颗粒剂 (1)本品为板蓝根制成的颗粒剂.(2)鉴别方法①取本品0.5g,加5ml甲醇使溶解,静置,取上清液点于滤纸上,晾干,置紫外光灯(365nm)下观察.②取本品0.5g,加10ml甲醇使溶解,滤过,取滤液1ml,加茚三酮试液0.5ml,置水浴中加热数分钟,观察颜色. Evaluation only. Created with Aspose.Slides for .NET 3.5 Client Profile 5.2.0.0. Copyright 2004-2011 Aspose Pty Ltd. 四、实验结果 药物名称 现象变化 牛黄解毒片 丹参片 穿心莲片 银黄口服液 板蓝根颗粒剂 Evaluation only. Created with Aspose.Slides for .NET 3.5 Client Profile 5.2.0.0. Copyright 2004-2011 Aspose Pty Ltd.