正丁醇常数法快速测定煎炸油脂中羰基价-食品安全质量检测学报.PDF

5 11 Vol. 5 No. 11 2014 11 Journal of Food Safety and Quality Nov. , 2014 1 1* 1 2 3 1 韩瑞阳 , 蓝 芳 , 梁 宏 , 刘 利 , 蔡 琳 , 侯乐锡 (1. , 518045; 2. , 430060; 3. , 518055) 摘 要: 目的 方法 , , 结果 , 88%~127%, 1.92%~9.82%结论 , 关键词: ; ; ; Rapid determination of carbonyl value in frying oils by 1-butanol constant method 1 1* 1 2 3 1 HAN RUI-Yang , LAN Fang , LIANG Hong , LIU Li , CAI Lin , HOU Le-Xi (1. Food Inspection and Quarantine Center, Shenzhen Entry-Exit Inspection and Quarantine Bureau, Shenzhen 518045, China; 2. Hubei Grain Oil Food Quality Supervision and Inspection Station , Wuhan 430061, China; 3. Shenzhen Academy of Metrology and Quality Inspection, Shenzhen 518055, China) ABSTRACT: Objective To determine carbonyl value in frying oils quickly and safely. Method A 1-butanol constant method was developed, 1-butanol was used as solvent to replace benzene, converted colo- rimetric absorbance into carbonyl value directly by measuring constant formula. Results The recovery rates of carbonyl compound were 88% to 127%, and the relative standard deviation were 1.92% to 9.82%. Conclu- sion Compared with the national standard method, this method which is suitable for the determination of carbonyl value in frying oils, is rapid, simple, precise and accurate. KEY WORD