原子吸收光谱法测定底栖动物重金属元素的含量.pdfVIP

第22 卷第4 期 江苏科技大学学报{自然科学版) Vol. 22 No.4 2∞8 年8 月 Journal of Jiangsu University of Science and Technology( Natural Scíence Editíon) Aug. 2∞8 原子吸收光谱法测寇底栖动物重金属元素的含量 盛建臣，智锁红，葛建强，万学峰 {江苏科技大学材料科学与工程学院，江苏镇江212∞3) 摘 要:测定了3 种底栖动物中隶、铅、锋、锅、顿和链的含量，将底格动物经烘干研磨制成粉，经硝酸-高氯酸消解后， 用原子吸收光谱法测定其中重金属元素的含量.实验发现:无需分离，即可用原子吸收法对重金属进行分析:经测定3 种 展栖动物中隶、铅、络、铜、锁和锚的含量多数超过国标.结果表明该方法简便、快速、醋试灵敏度高、线性关系良好、分析 准确，加标回收率达94. ∞号奋斗06. ∞%. 关键词:蔬幢动物;重金属;食品安全:富集;测定 中图分类号: TS207. 5+ 1 文献衍、i只码:A 文章编号: 1673 -4807(2∞8)04 -∞81 -05 Method to determine contents of heavy metal in zoobenthos with flame atomic absorption spectrometry SHENG Jíanguo , ZHI Suohong , GE Jianqiang , WAN Xuefeng (Schω.1 of Materials Science and Engineeri吨. Ji船gsu Uni回，ity of Science and Technol啼， Zhenjiang Ji凯gsu 212∞3 ， China) Abslract: This paper used flame atomic absorption spectrometry methods to determine the contents of Hg , 岛， Cr , Cu , Mn and Ba in three z∞benth础. Mter being dryed and grinded into powder , and being dissipated into solution with nitric acid and perchloric acid , the contents of heavy metal in zoobenthos was determined with flame atomic ahsorption spectrometry methods. 咀le experiment results indicatet the contεnts of Hg , Pb , Cr , Cu , Mn and Ba are higher than Nation Standaro. And heavy metal can be analyzed with alomic absorption method without the need to separate with one other. 古1εmethod proposed in this paper shows several advanta- ges such as high 旬到 sensitivity ， good linear relations , accurate analysis , the recove巧 reachs 94. 00% 阳 106.00%. Key words: zoobenthos; heavy metal; food safety; enrichmer址; determination 8 号 i 重金属污染是水体污染的一种影式，它可以通过富集在生物体内积票，最终通过食物进入人体，影 响人们的健康[IJ 然而，人们对各