甲醇精馏考试题（Methanol distillation test）.docVIP

甲醇精馏考试题（Methanol distillation test） Alcohol ether workshop rectification test 1. The national standard of excellent product methanol requires that the content of free acid is less than or equal to? 0.0015% 2. The contents of free alkali are less than or equal to the content of the national standard. 0.0002% In the methanol fractionate, the content of methanol is less than what? 0.3% 4. What is the PH value of the methanol rectification wastewater? 9 to 11 5. What are the main factors affecting the operation of the rectification tower during normal production? Answer: the amount of incoming flow rate is the quantity of the reboiler heating 6. What are the main factors affecting the liquid level of the distillation tower during normal production? Answer: return flow. Amount of incoming material. The distillation column reboiler heats the steam. Operating pressure of the rectification tower. Temperature of rectification tower kettle. The discharge of the liquid in the stilling of the cauldron 7. What are the main causes of excessive levels of light in the discharge fluid of the tower in the rectification operation? Low temperature of tower kettle Why does the pre-tower feed from the top? Because the pre-tower is mainly the removal of the light component, from the upper feeding, it is beneficial to the removal of light components. 9. What is the role of the fractionation section? Main task is to remove the water contained in the crude methanol, dimethyl ether, paraffin, higher alcohols and dissolved gas impurities, resulting in accord with GB338-2004 standard of the fine methanol product and by-product fusel alcohol at the same time sent to the fusel cans, methanol to wastewater biochemical treatment. What kind of material does the standing tower release? Ethanol-oil refined methanol waste water Why shut off the exit valve when the centrifugal pump is started? In order to unload the motor load, avoid causing tripping and even damage the equipment due to excessive curren