原创力文档Analysis of organic pollutants in water at trace levels using fully automated solid-phase extraction coupled to high-performance liquid chromatography：（分析有机污染物在水中的微量使用全自动固相萃取与高效液相色谱法）.pdfVIP
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Analysis of Organic Pollutants in Water at Trace Levels using
Fully Automated Solid-Phase Extraction Coupled to High-
Performance Liquid Chromatography
T. R e n n e r *1 / D. Baumgarten 1 / K. K. Unger 2
1Hessische Landesanstalt far Umwelt, Dez. III/2, P.O. Box 3209, 65022 Wiesbaden, Germany
2Institut fur Anorganische Chemic und Analytische Chemic, Johannes-Gutenberg Universit~it, 55099 Mainz,
Germany
Key Words
for fast screening of organic pollutants from three fifty-
Column liquid chromatography
millilitre aqueous samples are described.
Environmental trace analysis
Solid-phase extraction
Pesticides
Explosives Introduction
Polycyclic aromatic hydrocarbons
Thermally assisted desorption Liquid separation techniques are increasingly employed
in modern environmental analysis [1].Because it is nec-
essary to reduce the analytical uncertainty to less than
Summary 25 % of the sampling uncertainty [2], poor analytical re-
suits, particularly as a result of operator error (errors in
A method has been developed for the determination of procedure, confusion of reagents, contamination, etc.
t~ace levels of 32 pesticides, 19 explosives and 16 poly- [3]) must be avoided, or at least reduced. Automation of
cyclic aromatic hydrocarbons (PAH) in water in three the analytical method is, therefore, inevitable.
individual steps. Solid-phase enrichment (SPE) is cou-
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