Analysis of some anhydrides as their corresponding acids by capillary electrophoresis:(分析毛细管电泳的一些酐作为相应的酸).pdfVIP

Analysis of some anhydrides as their corresponding acids by capillary electrophoresis:(分析毛细管电泳的一些酐作为相应的酸).pdf

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Analysis of Some Anhydrides as Their Corresponding Acids by Capillary Electrophoresis Y. He / H. K. Lee* Department of Chemistry, National University of Singapore, Kent Ridge, Republic of Singapore 119260 hydrides are also present as pollutants in the workplace Key Words [9]. Direct determination of anhydrides is often difficult owing to their susceptibility to hydrolysis. Most pub- Capillary electrophoresis lished procedures for direct measurements use spectro- Reversed electroosmotic flow photometric techniques, e.g. IR and NMR spectrometry Organic acids [10, 11] to monitor functional groups. Direct normal- Anhydrides phase and reverse-phase HPLC methods for the deter- mination of some anhydrides were also reported re- cently [12, 13]. Indirect techniques such as titration, Summary spectrophotometry, gas chromatography and liquid chromatography involve hydrolysis and derivatization The potential of capillary electrophoresis for the indi- [14, 151. rect determination of anhydrides was demonstrated by The main purpose of the present study was to explore the analysis of five closely-related anhydrides as their

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