Analysis of some anhydrides as their corresponding acids by capillary electrophoresis:(分析毛细管电泳的一些酐作为相应的酸).pdfVIP
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Analysis of Some Anhydrides as Their Corresponding Acids
by Capillary Electrophoresis
Y. He / H. K. Lee*
Department of Chemistry, National University of Singapore, Kent Ridge, Republic of Singapore 119260
hydrides are also present as pollutants in the workplace
Key Words [9]. Direct determination of anhydrides is often difficult
owing to their susceptibility to hydrolysis. Most pub-
Capillary electrophoresis lished procedures for direct measurements use spectro-
Reversed electroosmotic flow photometric techniques, e.g. IR and NMR spectrometry
Organic acids [10, 11] to monitor functional groups. Direct normal-
Anhydrides phase and reverse-phase HPLC methods for the deter-
mination of some anhydrides were also reported re-
cently [12, 13]. Indirect techniques such as titration,
Summary spectrophotometry, gas chromatography and liquid
chromatography involve hydrolysis and derivatization
The potential of capillary electrophoresis for the indi- [14, 151.
rect determination of anhydrides was demonstrated by
The main purpose of the present study was to explore
the analysis of five closely-related anhydrides as their
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