原创力文档Analysis of sterols in vegetable oils using off-line SFCcapillary GC-MS：（分析使用离线SFCcapillary gc - ms固醇的植物油）.pdfVIP
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Analysis of Sterols in Vegetable Oils Using Off-Line SFC /
Capillary GC-MS
A. Medvedovicil/E David 2 / P. Sandra 1.
1Department of Organic Chemistry, University of Gent, Krijgslaan 281 S-4, 9000 Gent, Belgium
2Research Institute for Chromatography, Kennedypark 20, 8500 Kortrijk, Belgium
[3]. Both approaches are prone to irreproducibility and
Key Words are, above all, time-consuming.
The on-line coupling of LC with capillary GC allows
Supercritical fluid chromatography
removal of the triglyceride matrix and other interfering
Capillary GC-MS
Off-line fractionation compounds in a far more effective way [4-6]. The proce-
Sterol fraction dure includes a derivatisation reaction with pivalic acid
of the total oil, fractionation of the derivatised oil by
Vegetable oils
straight phase LC on silicagel using hexane, hexa-
ne/20 % dichloromethane/0.05 % acetonitrile, or hexa-
ne/3 % methyl t.butyl ether as mobile phase and back-
Summary flush after elution of the relevant fraction. The mobile
The analysis of sterols in vegetable oils by off-line SFC phase composition has to be adapted to the activity of
followed by capillary GC-MS is described. The frac- t
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