结晶和重结晶的操作步骤（Operation steps of crystallization and recrystallization）.docVIP

结晶和重结晶的操作步骤（Operation steps of crystallization and recrystallization） Its hard to love someone. Its harder to hate someone. Its the hardest thing to love and hate. Love can never be a balance, want to be happy in love to be sad! Some of our troubles are imaginary, but we take it as real. Operation steps of crystallization and recrystallization Crystallization and recrystallization include the following major steps: 1. The purified chemical reagent will need to be dissolved in boiling or in a suitable solvent for boiling; 2. Remove the insoluble impurities by draining the hot solution while it is hot. 3. Cooling the filtrate to precipitate the crystallization; 4. Filter out the crystallization and wash the crystals with appropriate solvent when necessary. The following problems should be noted in the operation of crystallization and recrystallization. 1. In advance to dissolve and purification of chemical reagents to strictly abide by the laboratory safety operational procedures, solvent heating inflammable, explosive, operation should be in the absence of open environment, and should avoid direct heat. Because in normal circumstances, solubility curve rises steeply at the boiling point of the solvent, so the solvent should be heated to the boiling point during crystallization and recrystallization. To make crystallization and recrystallization in high yield, the amount of solvent is as low as possible, so you start to join the amount of solvent to dissolve purification of chemical reagents, in the process of heating can be adding solvent, until when boiling dissolve solid matter. When adding solvent, it should be noted that if the solution is cooled to its boiling point, the explosion-proof zeolite will not be effective and the new zeolite needs to be added. 2. To quantitatively evaluate the operation of crystallization and recrystallization, and to facilitate repetition, both solids and solvents should be weighed and measured. 3. When using mixed solvent crystalliz