年产1500 吨仲钨酸铵的碱分解生产车间毕业设计.doc

摘 要 本文是以黑钨精矿钨矿原料年产1500吨APT（仲钨酸铵）生产车间的设计说明书。按照一般有色冶金生产车间设计步骤，文章首先概述APT生产的现状；结合原料特征，通过对APT整个工艺过程生产方法的比较，选择了苛性钠压煮法分解黑钨精矿—离子交换法除杂和转型—选择沉淀法分离钨钼—连续蒸发结晶生产APT的工艺。根据所选的工艺特点以及黑钨矿的分布特点,选择了黑钨矿储量丰富的粤北地区阳山县作为厂区地址。通过对各生产工序金属平衡、物料平衡计算和设备选型，确定了各工序所需原料的量和设备的型号、规格和数目，并进行了合理的车间配置。通过分析生产过程中工业三废的来源和危害，提出了三废处理的方案；根据生产过程需要，对车间进行了劳动定员。通过对整个工艺过程的技术经济分析，计算结果表明本设计所采用工艺流程技术上可行，经济上合理。投资回收期仅1.43年。 关键词： 钨；黑钨精矿；APT；分解；浸出；离子交换；结晶；设计 Abstract The specification is a workshop of 1500t a year ammonium paratungstate(APT) produced with wolframite concentrates．Following the general design steps of nonferrous metallurgy workshop，the present situation of the APT production was first presented．According to the characteristics of the raw material，technological process of caustic soda leaching at high pressure—ion exchange—selectively precipitation to separate Mo—evaporation and crystallization process was selected as the process of APT production. According to the characteristics of the selected technology, as well as the distribution of wolframite，Yangshan County in northern Guangdong with rich wolframite reserves was chosen as the site address．The quantity of various materials in every process were fixed up and the corresponding equipments were designed or selected（include the type， size and number）originated from the result of calculating of the balance of metal and matter． The workshop is reasonably designed．The strategy of dealing with the industrial waste was proposed following the analysis of the source and the harm of the waste．The work force was arranged according to the requirement of producing process．At last，the economic target was analyzed．All these results shows that the process of this design is reasonable and economical．The investment recoupment period is only 1.43 years． Keywords: tungesten wolframite concentrates；ammonium paratungstate；decompersition；leaching；ion exchange；crystallization；design 目录 TOC \o 1-3 \h \z \u HYPERLINK \l _Toc223361712 摘 要 PAGEREF _Toc223361712 \h 2 HYP