乳痛消结颗粒中4味药材的薄层色谱鉴别（TLC identification of 4 medicinal herbs in the milk of eliminating pain and resolving stasis）.docVIP

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乳痛消结颗粒中4味药材的薄层色谱鉴别（TLC identification of 4 medicinal herbs in the milk of eliminating pain and resolving stasis）.doc

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乳痛消结颗粒中4味药材的薄层色谱鉴别（TLC identification of 4 medicinal herbs in the milk of eliminating pain and resolving stasis）

乳痛消结颗粒中4味药材的薄层色谱鉴别（TLC identification of 4 medicinal herbs in the milk of eliminating pain and resolving stasis） TLC identification of 4 medicinal herbs in the milk of eliminating pain and resolving stasis Update Date: 06-19: Hou Juan, Zhang Lantong, Yuan Zhifang, Liu Jiang, Niu Yufeng Keywords Radix Salviae Miltiorrhizae; Radix Paeoniae Alba; Herba Epimedii; Radix Angelicae sinensis; isolation and purification; chromatography; TLC; Rutongxiaojie granules is a effective prescription in our hospital treatment of breast hyperplasia after years of clinical practice developed, consisting of 15 herbs in kelp, Salvia miltiorrhiza, Radix Paeoniae Alba, Radix Angelicae sinensis, epimedium, with Ruanjiansanjie, Shuganjieyu, Huoxue Tiaojing, pain Qi, yang meridians. In order to control its quality, radix salviae miltiorrhizae, Paeonia lactiflora pall, epimedium and Angelica sinensis were identified by tlc. 1 materials and methods 1.1 instrument and reagent 1.1.1 instrument TLC cylinder type P-1 (Shanghai Xinyi instrument factory); silica gel G plate (Yantai Chemical Industry Research Institute). 1.1.2 reagent of tanshinone A control (Chinese Institute for drug control, batch number: 766-9204); paeoniflorin reference (China Institute for drug control, batch number: 110736-200320); icariin standard (Chinese Institute for drug control, batch number: 110737-200312); ethyl ether, ethanol, 50% ethanol, 95% ethanol and other reagents are chemically pure; Salvia miltiorrhiza, Radix Paeoniae Alba, Herba Epimedii, angelica control medicinal materials provided by Shijiazhuang lerentang medicine plant; Rutongxiaojie granules made for the hospital preparation room. 1.2 TLC identification Identification of 1.2.1 Angelica 1.2.1.1 for sample preparation Rutongxiaojie granules 10 g, porphyrized, ether plus 10 mL, shaking, place a few hours, filtration, the filtrate was dried with anhydrous ethanol, the residue 1 mL dissolved, as the testsolution. 1.2.1.2 control medicine solution preparation